Methods for Surface Extraction of Food Surfaces
An innovative surface extraction and mass spectrometry system allows for rapid, cost-effective, and automatable on-site lipid analysis in food products without sample pre-processing.
In many food industries, lipid extraction to test for quality assurance and for special labeling is an essential part of the pre-market production process. There are a number of techniques designed to extract and analyze compounds found in food, such as liquid chromatography coupled with mass spectrometry. While effective, these methods are laboratory-based, time-consuming and expensive. Researchers at Purdue University have developed a new method of surface extraction coupled with mass spectrometry compatible with on-site and online mass spectrometry analysis, allowing for quick and cost-effective analysis. This innovative system increases speed and allows for a larger volume of testing while decreasing the need for employee training. The process can be automated using a robotic arm, which could streamline the process and be integrated into the product processing in industrial settings.
Technology Validation:
The sample extraction method was used to conduct lipidomic profiling of pre-freezing and post-freezing beef and chicken breast samples and red and brown beef samples
Advantages:
-Increased speed and efficiency of lipid analysis in food products
-Decreased employee training time
-Possibility of automation through use of a robotic arm
-Accurate and convenient analysis through online or offline mass spectrometry
-No need for sample pre-processing
Applications:
-Various food industries, particularly beef, in which on-site lipid analysis is used in grading and special labeling/categorization
TRL: 3
Intellectual Property:
Provisional-Patent, 2024-04-24, United States | PCT-Patent, 2025-04-23, WO
Keywords: Lipid extraction, Quality assurance, Food testing, Surface extraction, Mass spectrometry, On-site analysis, Online analysis, Cost-effective lipid analysis, Food industry applications, Robotic automation, Agriculture, Chemistry and Chemical Analysis, Food Products, Lipid panels, Mass Spectrometry, MRM profiling, Surface extraction