Formulation for Controlled Dispersion of Cellulose Nanomaterials

A new polymer shear mixing process using carboxymethylcellulose enables controlled dispersion and improved, homogenous drying of sustainable cellulose nanomaterials, overcoming traditional agglomeration issues.
Technology No. 2021-YOUN-69372

Researchers at Purdue University have created new process for controlled dispersion of cellulose nanomaterials using carboxymethylcellulose. Cellulose nanomaterials materials are desirable as they are sustainable, biodegradable, and highly abundant in nature. CNCs can be used in cosmetic, composite, paint, ink, gas, packaging, construction, and food applications – to name a few. Currently, agglomeration of CNCs can occur as they are dried, and processes used to reduce this effect traditionally involve costly, energy-intensive methods as well as often compromise material properties. Purdue researchers have combined a polymer shear mixing technique to create CNC and a CMC dispersion that allows for redispersion the material. The technique can also hinder redispersion as desired by soaking the dispersion in multi-valent salt solutions or dilute acids. Further, this improves the material's ability to dry evenly and homogenously.

Advantages:

-Sustainable Materials

-Improved Drying Step in CNC/CMC Material Development

Potential Applications:

-Material Science and Engineering

-Composites

-Construction

-Packaging

Technology Validation:

The charge potential was tested for pure CNC versus the CNC + CMC mixture at various stages in the drying process.

Recent Publication:

"Enhanced dispersion and properties of a two-component epoxy nanocomposite using surface modified cellulose nanocrystals"

Polymer, a journal of Materials Today

DOI: 10.1016/j.polymer.2017.02.016​

TRL: 3

Intellectual Property:

Provisional-Patent, 2021-03-15, United States | NATL-Patent, 2022-03-15, Finland | PCT-Patent, 2022-03-15, WO | NATL-Patent, 2022-03-15, Canada | NATL-Patent, 2022-03-15, United Kingdom | Utility Patent, 2022-03-15, United States | CON-Gov. Funding, 2025-09-09, United States

Keywords: Cellulose nanomaterials, carboxymethylcellulose, controlled dispersion, CNC, CMC, polymer shear mixing, redispersion, sustainable materials, composites, packaging, Carbon Nanotubes, Composites, Construction, Construction Technologies, Materials and Manufacturing, Materials Science, Mechanical Engineering, packaging

  • expand_more mode_edit Authors (5)
    Sami El Awad Azrak
    Endrina Forti
    Robert Moon
    Gregory Schueneman
    Jeffrey P Youngblood
  • expand_more cloud_download Supporting documents (1)
    Product brochure
    Formulation for Controlled Dispersion of Cellulose Nanomaterials.pdf
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